4,4,5,5-四甲基-1,3,2-二氧磷杂环戊烷-2-醇合成路线 (共 23 条)
反应条件
in toluene 25 h; Heating;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 51, # 5 p. 999 - 1002,834 - 837
反应条件
[rhodium(I)chloride(triphenylphosphine)3] in acetone
T=25°C; P=760 Torr; 20 h;
参考文献
Zhao, Chang-Qiu; Han, Li-Biao; Goto, Midori; Tanaka, Masato
Angewandte Chemie - International Edition, 2001 , vol. 40, # 10 p. 1929 - 1932
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in toluene
T=90 - 100°C;
参考文献
Maffei, Michel; Buono, Gerard
Tetrahedron, 2003 , vol. 59, # 44 p. 8821 - 8825