(R)-1-苯基-1,2-乙二醇合成路线 (共 159 条)
反应条件
1: toluene; diethyl ether / 0.42 h / -20 °C 2: Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 17 p. 5595 - 5607
反应条件
1: toluene; diethyl ether / 0.42 h / -20 °C 2: Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 17 p. 5595 - 5607
反应条件
1: toluene; diethyl ether / 0.42 h / -20 °C 2: Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 17 p. 5595 - 5607
反应条件
1: 73 percent / pyridine; DMAP / 2 h / 20 °C 2: HgCl2 / acetonitrile; H2O / 3 h / 20 °C 3: 12 mg / LiAlH4 / diethyl ether / 2 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 5 p. 1581 - 1589
反应条件
1: HgCl2 / acetonitrile; H2O / 3 h / 20 °C 2: 12 mg / LiAlH4 / diethyl ether / 2 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 5 p. 1581 - 1589
反应条件
1: 6 percent / sucrose / H2O / 8 h / Ambient temperature; bakers' yeast 2: 85 percent / sucrose / H2O / 168 h / 30 °C / bakers' yeast View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 18 p. 4405 - 4407
反应条件
1: 80 percent / calcium sulfate / various solvent(s) / 0.5 h / 100 °C 2: 4 percent / sucrose / H2O / 8 h / Ambient temperature; bakers' yeast 3: 85 percent / sucrose / H2O / 168 h / 30 °C / bakers' yeast View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 18 p. 4405 - 4407
反应条件
Colletotrichum crassipes; PDB medium in ethanol T=25°C; 240 h; Microbiological reaction; optical yield given as percent ee;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 23 p. 2666 - 2672
反应条件
Bacillus subtilis ECU0554 esterase-expressing Escherichia coli BL21 in ethanol T=35°C; pH=7.5; 0.75 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 73, # 1-4 p. 80 - 84
反应条件
1: pyridine; 4-dimethylaminopyridine / 3 h / 20 °C 2: aq. HgCl2 / acetonitrile / 6 h / 20 °C 3: LiAlH4 / tetrahydrofuran / 3 h / 0 - 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 15 p. 2168 - 2169