(R)-1-苯基-1,2-乙二醇合成路线 （共 159 条）
反应条件
sodium tetrahydroborate; ozone Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 28, # 43 p. 5145 - 5148
反应条件
1: With lithium aluminium tetrahydride 2: With N-chloro-succinimide; silver nitrate 3: With sodium tetrahydroborate Further stages.;
参考文献
Tetrahedron Letters, , vol. 45, # 10 p. 2141 - 2145
反应条件
manganese sulphate; Jacobsen's (S,S)-(salen)Co(III) catalyst; water; dihydrogen peroxide; sodium hydrogencarbonate; acetic acid; urea optical yield given as percent eeenantioselective reaction;
参考文献
Green Chemistry, , vol. 12, # 5 p. 815 - 827
反应条件
sodium hydroxide 1.) reflux, 1.5 h, 2.) MeOH, r.t., overnight; 50 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Agricultural and Biological Chemistry, , vol. 46, # 5 p. 1153 - 1157
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 15, # 19 p. 3059 - 3072
反应条件
in ethanol; water T=30°C; 168 h; Bacillus subtilis subsp. niger IFO 3108, on nutrient agar plates pH 7.0; other solvents, other microorganisms; stereoselectivity; Product distributionMechanism;
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 8 p. 1216 - 1220
反应条件
1: 91 percent / DMAP; Et3N / CH2Cl2 / 2 h / 20 °C 2: 85 percent / t-BuOK / acetonitrile / 12 h / 20 °C 3: 100 percent / TBAF / acetonitrile / 4 h / 20 °C 4: 79 percent / TEMPO; NaClO; NaClO2 / acetonitrile; aq. phosphate buffer / 4 h / 55 °C View Scheme
参考文献
Moreno-Dorado, F. Javier; Guerra, Francisco M.; Ortega, Maria J.; Zubia, Eva; Massanet, Guillermo M.
Tetrahedron Asymmetry, 2003 , vol. 14, # 4 p. 503 - 510
反应条件
zirconium tetrachloride in dichloromethane T=25°C; 2 h; Title compound not separated from byproducts.;
参考文献
Singh, Surendra; Duffy, Colm D.; Shah, Syed Tasadaque A.; Guiry, Patrick J.
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6429 - 6432
反应条件
pyridine T=-10°C; 4 h;
参考文献
Uccello-Barretta, Gloria; Cuzzola, Angela; Balzano, Federica; Menicagli, Rita; Iuliano, Anna; Salvadori, Piero
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 827 - 835
反应条件
1: 91 percent / DMAP; Et3N / CH2Cl2 / 2 h / 20 °C 2: 85 percent / t-BuOK / acetonitrile / 12 h / 20 °C 3: 100 percent / TBAF / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Wu, Guang-Peng; Zu, Yu-Ping; Xu, Peng-Xiang; Ren, Wei-Min; Lu, Xiao-Bing
Chemistry - An Asian Journal, 2013 , vol. 8, # 8 p. 1854 - 1862
