1,4-二甲氧基-2-丁炔合成路线 （共 33 条）
反应条件
2,3,4,5-tetrakis(carbomethoxy)-spiro-glyoxalbis(2,6-diisopropylphenylimine)palladacyclopenta-2,4-diene in toluene T=80°C; 22 h;
参考文献
Dieck, Heindirk tom; Munz, Christina; Mueller, Christiane
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 243 - 255
反应条件
copper(I) bromide in diethyl ether T=0°C; 2 h; Yields of byproduct given;
参考文献
Ishino, Yoshio; Nishiguchi, Ikuzo; Takihira, Fujio; Hirashima, Tsuneaki
Tetrahedron Letters, 1980 , vol. 21, p. 1527 - 1528
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Koshino, Junji; Sugawara, Takahiro; Suzuki, Akira
Synthetic Communications, 1984 , vol. 14, # 3 p. 245 - 250
反应条件
trimethylsilylazide T=114°C; 240 h;
参考文献
Banert, Klaus
Chemische Berichte, 1989 , vol. 122, p. 911 - 918
反应条件
copper(I) bromide in diethyl ether
T=0°C; 2 h; Yields of byproduct given;
参考文献
Ishino, Yoshio; Nishiguchi, Ikuzo; Takihira, Fujio; Hirashima, Tsuneaki
Tetrahedron Letters, 1980 , vol. 21, p. 1527 - 1528
反应条件
in diethyl ether
1.) r.t., 30 min, 2.) reflux, 2 h;
参考文献
Silva, Anthony N. De; Francis, Craig L.; Ward, A. David
Australian Journal of Chemistry, 1993 , vol. 46, # 11 p. 1657 - 1672
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Koshino, Junji; Sugawara, Takahiro; Suzuki, Akira
Synthetic Communications, 1984 , vol. 14, # 3 p. 245 - 250
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Koshino, Junji; Sugawara, Takahiro; Suzuki, Akira
Synthetic Communications, 1984 , vol. 14, # 3 p. 245 - 250
反应条件
copper(I) bromide in diethyl ether
T=0°C; 2 h;
参考文献
Ishino, Yoshio; Nishiguchi, Ikuzo; Takihira, Fujio; Hirashima, Tsuneaki
Tetrahedron Letters, 1980 , vol. 21, p. 1527 - 1528
反应条件
n-butyllithium; acetic acid
Yield given. Multistep reaction;
参考文献
Koshino, Junji; Sugawara, Takahiro; Suzuki, Akira
Heterocycles, 1984 , vol. 22, # 3 p. 489 - 492
