1,4-二甲氧基-2-丁炔合成路线 (共 33 条)
反应条件
1: aqueous methanol; mercury (II)-oxide; sulfuric acid
2: sodium acetate / 150 °C / 100 - 150 Torr
View Scheme
参考文献
Mazojan et al.
Izvestiya Akademii Nauk Armyanskoi SSR, Khimicheskie Nauki, 1959 , vol. 12, p. 187,190
Chem.Abstr., 1960 , p. 7545
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Koshino, Junji; Sugawara, Takahiro; Suzuki, Akira
Synthetic Communications, 1984 , vol. 14, # 3 p. 245 - 250
反应条件
copper(I) bromide in diethyl ether
T=0°C; 2 h; Yields of byproduct given;
参考文献
Ishino, Yoshio; Nishiguchi, Ikuzo; Takihira, Fujio; Hirashima, Tsuneaki
Tetrahedron Letters, 1980 , vol. 21, p. 1527 - 1528