2-(3-硝基苯氧基)乙醇合成路线 (共 8 条)
反应条件
potassium carbonate in acetonitrile 24 h; Reflux;
参考文献
Hashim; Thomas, Reji; Tamaoki, Nobuyuki
Chemistry - A European Journal, 2011 , vol. 17, # 26 p. 7304 - 7312
反应条件
sodium hydroxide auf Siedetemperatur;
参考文献
Mamedov,S.; Alieva,Kh.M.
Journal of Organic Chemistry USSR (English Translation), 1967 , vol. 3, p. 1421 - 1426
Zhurnal Organicheskoi Khimii, 1967 , vol. 3, p. 1462 - 1468
反应条件
tetraethylammonium bromide T=180°C; 1 h;
参考文献
Sternson, L. A.; Chandrasakar, R.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4295 - 4297
反应条件
in N,N-dimethyl-formamide 11 h; Heating;
参考文献
Wubbels, Gene G.; Halverson, Ann M.; Oxman, Joe D.; Bruyn, Van H. De
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4499 - 4504
反应条件
ethanol; sodium ethanolate
参考文献
Boyd; Marle
Journal of the Chemical Society, 1914 , vol. 105, p. 2123
参考文献
Boyd; Marle
Journal of the Chemical Society, 1914 , vol. 105, p. 2123
反应条件
hydrazine hydrate in methanol; water T=50°C; 2.41667 h; Reflux;
参考文献
Chepyshev; Chepysheva; Ryabitskii; Prosyanik
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 5 p. 523 - 529
Khim. Geterotsikl. Soedin.
反应条件
1: 72 percent / pyridine / 24 h
2: 72 percent / dimethylformamide / 1 h / 100 °C
3: 61 percent / aq. HCl / acetic acid / 16 h / Heating
4: 75 percent / 0.01 M aq. NaOH / 6 h / Irradiation; var. triplet sensitizers; photochemical Smiles rearrangement
View Scheme
参考文献
Wubbels, Gene G.; Halverson, Ann M.; Oxman, Joe D.; Bruyn, Van H. De
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4499 - 4504