苯并咪唑并[1,2-c]喹唑啉-6(5h)-酮合成路线 （共 18 条）
反应条件
titanium tetrachloride; zinc in tetrahydrofuran
T=20°C; Inert atmosphereReflux;
参考文献
Zhao, Xuan; Shi, Da-Qing
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 3 p. 524 - 527
参考文献
Molina, Pedro; Alajarin, Mateo; Vidal, Angel
Tetrahedron, 1989 , vol. 45, # 13 p. 4263 - 4286
反应条件
sodium methylate in methanol
4 h; Heating;
参考文献
Rastogi, Rashmi; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 579 - 582
反应条件
1: 75 percent / DCC / CH2Cl2 / 1.) 0 deg C, 30 min, 2.) RT; 2 h,
2: 72 percent / AcONa / acetic acid / 1 h / Heating
3: 84 percent / AcONa / CH2Cl2; diethyl ether / 3 h / Ambient temperature
4: 76 percent / toluene / 12 h / 90 °C
View Scheme
参考文献
Molina, Pedro; Alajarin, Mateo; Vidal, Angel
Tetrahedron, 1989 , vol. 45, # 13 p. 4263 - 4286
反应条件
1: 75 percent / DCC / CH2Cl2 / 1.) 0 deg C, 30 min, 2.) RT; 2 h,
2: 72 percent / AcONa / acetic acid / 1 h / Heating
3: 84 percent / AcONa / CH2Cl2; diethyl ether / 3 h / Ambient temperature
4: 76 percent / toluene / 12 h / 90 °C
View Scheme
参考文献
Molina, Pedro; Alajarin, Mateo; Vidal, Angel
Tetrahedron, 1989 , vol. 45, # 13 p. 4263 - 4286
反应条件
in acetic acid
2 h; Heating;
参考文献
Padmaja, J.; Reddy, M. Satyanarayana; Ratnam, C. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 951 - 954
反应条件
1: 71.4 percent / tetrahydrofuran / 8 h / Heating
2: 86.9 percent / NaOMe / methanol / 4 h / Heating
View Scheme
参考文献
Rastogi, Rashmi; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 579 - 582
参考文献
Leistner; Wagner; Strohscheidt Th.
Pharmazie, 1980 , vol. 35, # 5-6 p. 293 - 296
参考文献
Leistner; Wagner; Strohscheidt Th.
Pharmazie, 1980 , vol. 35, # 5-6 p. 293 - 296
参考文献
Leistner; Wagner; Strohscheidt Th.
Pharmazie, 1980 , vol. 35, # 5-6 p. 293 - 296
