2-氨基-4,6-二甲氧基-1,3,5-三嗪合成路线 (共 11 条)
反应条件
ammonia in water T=25 - 51°C; 2 h;
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US6833454 B1, 2004 ;
Location in patent: Page column 6-7 ;
反应条件
ammonia; sodium methylate in methanol; water; toluene
参考文献
Novartis Corporation
Patent: US5721364 A1, 1998 ;
反应条件
manganese(IV) oxide in ethyl acetate 72 h; Heating;
参考文献
Katritzky, Alan R.; Dennis, Nicholas; Dowlatshahi, Hossein A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 331 - 342
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2986,2989
反应条件
acetophenone 48 h; Irradiation;
参考文献
Itahara, Toshio
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 1 p. 305 - 306
反应条件
1: 5 percent / benzene / Ambient temperature 2: 67 percent / SiO2 / column chromatography ( light petroleum - EtOAc) 3: 55 percent / manganese dioxide / ethyl acetate / 72 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 331 - 342
参考文献
Chemische Berichte, , vol. 3, p. 271
反应条件
in phosphate buffer T=20°C; 500 h; KineticsProduct distribution;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 50, # 5 p. 1081 - 1088
反应条件
1: 2-Amino-4,6-dimethoxy-1,3,5-triazine With hydrogen; sodium hydride in N,N-dimethyl acetamide T=20°C; 2: carbonic acid diphenyl ester in N,N-dimethyl acetamide 0.266667 h;
参考文献
KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
Patent: EP1209153 A2, 2002 ;
Location in patent: Example 2 ;
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4238621 A1, 1980 ;