2-碘-1,3-二异丙基苯合成路线 （共 6 条）
反应条件
1: With hydrogenchloride; sodium nitrite 2: With potassium iodide Further stages.;
参考文献
Hunter, Christopher A; Jones, Philip S; Tiger, Pascale M N; Tomas, Salvador
Chemical communications (Cambridge, England), 2003 , # 14 p. 1642 - 1643
反应条件
potassium iodide; sodium nitrite in hydrogenchloride; ligroin; water; ethyl acetate
参考文献
Jensen, Bo Skaaning; Teuber, Lene; Strobaek, Dorte; Christophersen, Palle; Olesen, Soren Peter
Patent: US2002/65315 A1, 2002 ;
反应条件
1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C 1.2: 0.5 h 2.1: Cu(OTf)2; potassium fluoride; 18-crown-6 ether / N,N-dimethyl-formamide / 18 h / 60 °C View Scheme
参考文献
Ichiishi, Naoko; Canty, Allan J.; Yates, Brian F.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 19 p. 5134 - 5137
反应条件
1: With copper(l) iodide; 1,10-phenanthroline; potassium hydroxide in water; dimethyl sulfoxide T=20 - 100°C; Inert atmosphere; 2: With hydrogenchloride in water; dimethyl sulfoxide T=20°C; Inert atmosphere;
参考文献
Zhao, Dongbing; Wu, Ningjie; Zhang, Shuai; Xi, Peihua; Su, Xiaoyu; Lan, Jingbo; You, Jingsong
Angewandte Chemie - International Edition, 2009 , vol. 48, # 46 p. 8729 - 8732
反应条件
1: 81 percent / n-BuLi
2: (COCl)2
View Scheme
参考文献
Hunter, Christopher A; Jones, Philip S; Tiger, Pascale M N; Tomas, Salvador
Chemical communications (Cambridge, England), 2003 , # 14 p. 1642 - 1643
反应条件
1: 2-iodo-1,3-diisopropylbenzene With n-butyllithium
2: carbon dioxide Further stages.;
参考文献
Hunter, Christopher A; Jones, Philip S; Tiger, Pascale M N; Tomas, Salvador
Chemical communications (Cambridge, England), 2003 , # 14 p. 1642 - 1643
