5,6-二甲氧基吲哚-2-甲酸乙酯合成路线 (共 16 条)
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=50°C; 4 h; Inert atmosphere;
参考文献
Cai, Qian; Li, Zhengqiu; Wei, Jiajia; Ha, Chengyong; Pei, Duanqing; Ding, Ke
Chemical Communications, 2009 , # 48 p. 7581 - 7583
反应条件
copper(I) oxide; caesium carbonate in 1-methyl-pyrrolidin-2-one T=100°C; 16 h; Inert atmosphereSealed tube;
参考文献
Zhu, Zhiqiang; Yuan, Jiangjun; Zhou, Yirong; Qin, Yang; Xu, Jingshi; Peng, Yiyuan
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 511 - 514
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=80°C; 16 h; Inert atmosphere;
参考文献
Koenig, Stefan G.; Dankwardt, John W.; Liu, Yanbing; Zhao, Hang; Singh, Surendra P.
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6549 - 6551
反应条件
triethyl phosphite T=170°C; 3 h;
参考文献
Mali; Yadav
Synthesis, 1984 , vol. NO. 10, p. 862 - 865
反应条件
1: 72 percent / 5 h / 90 °C 2: 71 percent / ZnCl2 / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Synlett, , # 5 p. 749 - 755
反应条件
1: K2CO3 / acetone / 12 h / 60 °C 2: 72 percent / 5 h / 90 °C 3: 71 percent / ZnCl2 / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Synlett, , # 5 p. 749 - 755
反应条件
1: sodium / methanol / -20 - 0 °C 2: anhydrous xylene / Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 34, # 3 p. 357 - 367
反应条件
ethanol; sodium acetate Kochen des oeligen Hydrazons mit alkoh. Salzsaeure;
参考文献
Journal of the Chemical Society, , p. 361
参考文献
Journal of the Chemical Society, , p. 2536
反应条件
in anhydrous xylene Reflux;
参考文献
Choi, Taeyoung; Ma, Eunsook
Archives of Pharmacal Research, 2011 , vol. 34, # 3 p. 357 - 367