反应条件
bromobenzene; water; calcium in gas
Ca vaporized at 900°C in vac. (ca. 5E-3 Torr), Me3SiSnMe3 introduced as vapor, mixed vapor condensed on cold (77 K) walls, warmed to room temp., excess of C6H5Br admitted as vapor, left to stand for 1 h, hydrolyzed with water; org. layer extd. with ether, products identified by GC-MASS, GLC;
参考文献
Mochida, Kunio; Yamanishi, Takayuki
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3429 - 3430
