2,3,3-三甲基-3H-吲哚合成路线 （共 91 条）
反应条件
1: toluene / 5 h / Heating 2: 95 percent / CHCl3 / Ambient temperature 3: 92 percent / hydrogen / W-2 Raney nickel / methanol / 760 Torr / Ambient temperature 4: 80 percent / 30percent hydrochloric acid / methanol / 25 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 46, # 23 p. 7865 - 7872
反应条件
1: 80 percent / 30percent hydrochloric acid / methanol / 25 h / Heating 2: 99 percent / Et3N / benzene / 24 h / Ambient temperature 3: 76 percent / hydrogen / W-2 Raney nickel / methanol / 760 Torr / Ambient temperature 4: toluene / 5 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 46, # 23 p. 7865 - 7872
反应条件
zinc(II) chloride in paraffin T=200 - 210°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Synthesis, , # 12 p. 958 - 959
反应条件
hydrogenchloride in methanol 25 h; Heating;
参考文献
Tetrahedron, , vol. 46, # 23 p. 7865 - 7872
反应条件
in diethyl ether 2.75 h; Irradiation;
参考文献
Hill, John; Zakaria, Marwan M.; Mumford, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2455 - 2458
反应条件
potassium permanganate
参考文献
Chemische Berichte, , vol. 31, p. 1496
Gazzetta Chimica Italiana, , vol. 28 II, p. 372
反应条件
in toluene 5 h; Heating;
参考文献
Malamidou-Xenikaki; Coutouli-Argyropoulou
Tetrahedron, 1990 , vol. 46, # 23 p. 7865 - 7872
反应条件
1: ZnCl2 / paraffin / 8 h / 200 - 210 °C 2: 85 percent / ZnCl2, LiCl / paraffin / 1.) 10 h, 190 degC, 2.) 6 h, 200 - 205 degC View Scheme
参考文献
Synthesis, , # 12 p. 958 - 959
反应条件
1: silica gel / CH2Cl2 / 48 h / Ambient temperature 2: 20 percent / 30percent hydrochloric acid / methanol / 25 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 46, # 23 p. 7865 - 7872
反应条件
silica gel in dichloromethane 48 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 46, # 23 p. 7865 - 7872
