2,3,3-三甲基-3H-吲哚合成路线 (共 91 条)
反应条件
1: 92 percent / 4 h / 100 °C 2: 35 percent / triethylamine / ethanol / 3 h / Heating View Scheme
参考文献
Li, Xiaoliu; Wang, Yongmei; Matsuura, Teruo; Meng, Jiben
Heterocycles, 1999 , vol. 51, # 11 p. 2639 - 2651
反应条件
in butanone T=140°C; 10 h;
参考文献
Elizalde, Luis Ernesto; Ledezma, Raquel; Lopez, Raul G.
Synthetic Communications, 2005 , vol. 35, # 4 p. 603 - 610
反应条件
1: acetonitrile / 15 h / Reflux 2: butan-1-ol; benzene / 10 h / 160 °C / Inert atmosphere View Scheme
参考文献
Kang, Nam-Young; Park, Sung-Jin; Ang, Xiao Wei Emmiline; Samanta, Animesh; Driessen, Wouter H. P.; Ntziachristos, Vasilis; Vasquez, Kristine O.; Peterson, Jeffrey D.; Yun, Seong-Wook; Chang, Young-Tae
Chemical Communications, 2014 , vol. 50, # 50 p. 6589 - 6591
反应条件
in nitromethane T=20°C; 12 h;
参考文献
Kiyose, Kazuki; Hanaoka, Kenjiro; Oushiki, Daihi; Nakamura, Tomomi; Kajimura, Mayumi; Suematsu, Makoto; Nishimatsu, Hiroaki; Yamane, Takehiro; Terai, Takuya; Hirata, Yasunobu; Nagano, Tetsuo
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15846 - 15848
反应条件
T=120°C; 0.75 h; Neat (no solvent)Microwave irradiation;
参考文献
Heller, Eberhard; Lautenschlaeger, Werner; Holzgrabe, Ulrike
Tetrahedron Letters, 2009 , vol. 50, # 12 p. 1321 - 1323
反应条件
in acetonitrile 48 h; Reflux;
参考文献
UNIVERSITY OF CENTRAL LANCASHIRE; OKOH, Okoh Adeyi; SMITH, Robert Bernard
Patent: WO2013/114115 A1, 2013 ;
Location in patent: Paragraph 00120 ;
反应条件
1: 1,2-dichloro-ethane / 5 h / 20 °C / Reflux 2: sodium hydroxide / water; acetone View Scheme
参考文献
KOREA UNIVERSITY RESEARCH AND BUSINESS FOUNDATION
Patent: US2011/198546 A1, 2011 ;
参考文献
Plancher
Chemiker-Zeitung, Chemische Apparatur, 1898 , vol. 22, p. 38
Chemische Berichte, 1898 , vol. 31, p. 1496
Full Text Show Details
Plancher
Gazzetta Chimica Italiana, 1898 , vol. 28 II, p. 426
反应条件
Yield given. Multistep reaction;
参考文献
Doepp, Dietrich; Rehmer, Gerd; Brueggemann, Helmut
Chemische Berichte, 1988 , vol. 121, p. 1651 - 1656
反应条件
Yield given. Multistep reaction;
参考文献
Doepp, Dietrich; Rehmer, Gerd; Brueggemann, Helmut
Chemische Berichte, 1988 , vol. 121, p. 1651 - 1656