2,1,3-苯并噻二唑-5-甲酸合成路线 (共 5 条)
反应条件
sodium hydroxide; silver nitrate
参考文献
Bulletin of the Chemical Society of Japan, , vol. 32, p. 551
反应条件
1: N-bromo-succinimide 3: aqueous acetic acid; hexamethylenetetramine 4: AgNO3; aqueous NaOH View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 32, p. 551
反应条件
2: aqueous acetic acid; hexamethylenetetramine 3: AgNO3; aqueous NaOH View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 32, p. 551
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 1570,1572; engl. Ausg. S. 1643, 1645
反应条件
1: With triethylamine; isobutyl chloroformate in tetrahydrofuran T=0°C; 0.5 h; 2: With sodium tetrahydroborate; water in tetrahydrofuran T=0°C; 0.5 h;
参考文献
SMITHKLINE BEECHAM P.L.C.
Patent: WO2003/87098 A1, 2003 ;
Location in patent: Page/Page column 39 ;