4-溴甲基-2,1,3-苯并噻重氮合成路线 （共 8 条）
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
The Ohio State University
Patent: US6376664 B1, 2002 ;
反应条件
N-bromosuccinmide in tetrachloromethane 3 h; HeatingIrradiation;
参考文献
Heterocycles, , vol. 45, # 5 p. 955 - 962
反应条件
1: 58 percent / Sn, concd. hydrochloric acid / H2O / 2.5 h / Heating 2: 74 percent / N-thionylaniline / toluene / 3 h / 80 - 100 °C 3: 71 percent / N-bromosuccinimide / CCl4 / 3 h / Heating; Irradiation View Scheme
参考文献
Heterocycles, , vol. 45, # 5 p. 955 - 962
反应条件
1: 74 percent / N-thionylaniline / toluene / 3 h / 80 - 100 °C 2: 71 percent / N-bromosuccinimide / CCl4 / 3 h / Heating; Irradiation View Scheme
参考文献
Heterocycles, , vol. 45, # 5 p. 955 - 962
反应条件
lithium salt of 2-nitropropane in methanol 24 h; Ambient temperature;
参考文献
Vanelle, Patrice; Liegeois, Celine Tremblais; Meuche, Jacobine; Maldonado, Jose; Crozet, Michel P.
Heterocycles, 1997 , vol. 45, # 5 p. 955 - 962
反应条件
1: (i) NaOEt, EtOH, (ii) /BRN= 1073116/, benzene 2: aq. HCl / Heating View Scheme
参考文献
Pesin,V.G.; D'yachenko,S.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1968 , vol. 4, p. 189 - 190
Khimiya Geterotsiklicheskikh Soedinenii, 1968 , vol. 4, p. 254 - 255
反应条件
silver perchlorate in 1,4-dioxane; hexane; water; ethyl acetate
参考文献
The Ohio State University
Patent: US6376664 B1, 2002 ;
反应条件
1: Et3N / benzene
2: HBr / benzene
3: aq. Na3PO3S / propan-2-ol
4: I2 / methanol; H2O
View Scheme
参考文献
Slavachevskaya,N.M. et al.
Pharmaceutical Chemistry Journal, 1979 , vol. 13, # 6 p. 591 - 598
Khimiko-Farmatsevticheskii Zhurnal, 1979 , vol. 13, # 6 p. 33 - 41
