in tetrahydrofuran Irradiation (UV/VIS); Fe complex and (13)CO in THF were photolyzed (black light bulb, emission max. 366 nm) at 15°C; react. monitored by (13C-NMR: solvent was removed, Cr(acac)3 was added and solid dissolved in benzene-d6;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 7106
in dichloromethane-d2 charging a NMR tube containing Zr-complex and CD2Cl2 with 1 atm of (13)CO at 23°C, mixing for 5 min; monitoring by (1)H-NMR, removal of solvent in vacuo;
Gasser, R. P. H.; Marsay, C. J.
Transactions of the Faraday Society, 1968 , vol. 64, p. 516 - 521
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Gmelin Handbook: Mo: SVol.A3, 2.6.17.1.4, page 138 - 141
catalyst: MoO3/SiO2 adsorption at 77 K, 30 Torr, heating at 140 K;
参考文献
Gonzalez-Elipe, Agustin R.; Louis, Catherine; Che, Michel
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1982 , vol. 78, p. 1297 - 1302
