2,2-二甲基丙基甲烷磺酸酯合成路线 （共 9 条）
反应条件
triethylamine in dichloromethane T=0°C; 2.5 h;
参考文献
Adamczyk, Maciej; Chen, Yon-Yih; Mattingly, Phillip G.; Pan, You; Rege, Sushil
Journal of Organic Chemistry, 1998 , vol. 63, # 16 p. 5636 - 5639
反应条件
sodium hydroxide in 1,4-dioxane; water 2 h; Heating;
参考文献
King, James F.; Gill, Manjinder S.
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7250 - 7255
反应条件
1: 2.) Et3N / 1.) CH2Cl2, room temperature, 30 min, 2.) 0 deg C, 15 min, room temperature, 30 min 2: 62 percent / 1 M NaOH / 18 h / Ambient temperature 3: 60 percent / NaOH / H2O; dioxane / 2 h / Heating View Scheme
参考文献
King, James F.; Gill, Manjinder S.
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7250 - 7255
反应条件
1: 62 percent / 1 M NaOH / 18 h / Ambient temperature 2: 60 percent / NaOH / H2O; dioxane / 2 h / Heating View Scheme
参考文献
King, James F.; Gill, Manjinder S.
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7250 - 7255
反应条件
1: 1 M aq. NaOH / dioxane / 11 h / Ambient temperature 2: 60 percent Spectr. / 1 M aq. NaOH / dioxane / 2 h / Heating View Scheme
参考文献
King, James F.; Gill, Manjinder Singh
Angewandte Chemie, 1995 , vol. 107, # 15 p. 1778 - 1780
反应条件
1: 75 percent / 1 M aq. NaOH / dioxane / 0.25 h 2: 6.6 M aq. NaOH / dioxane / 6 h / Heating View Scheme
参考文献
King, James F.; Gill, Manjinder Singh
Angewandte Chemie, 1995 , vol. 107, # 15 p. 1778 - 1780
反应条件
sodium hydroxide in 1,4-dioxane 6 h; Heating; Title compound not separated from byproducts;
参考文献
King, James F.; Gill, Manjinder Singh
Angewandte Chemie, 1995 , vol. 107, # 15 p. 1778 - 1780
反应条件
in dimethyl sulfoxide T=140°C; other solvents; Rate constantProduct distribution;
参考文献
Masada, Hiromitsu; Tajima, Katsuhiko; Taniguchi, Koichi; Yamamoto, Tomoya
Chemistry Letters, 1991 , # 5 p. 753 - 756
反应条件
in isopropyl alcohol
参考文献
GENERAL ELECTRIC COMPANY
Patent: EP126950 B1, 1991 ;
