反应条件
hydrogenchloride in ethanol KReO4 was refluxed in benzoyl chloride for 5 h, HCl saturated soln. of Bu4NBr in ethanol was added to a cooled mixture, refluxed for 1 h, underpositive pressure of N2; concn., addition of diethyl ether, filtration, washing a ppt. with ethanol and diethyl ether, addition of hot methanol, filtration into conc. HCl, evapn. by boiling, filtration, washing a ppt. with ethanol, Et2O, drying in vac.; elem. anal.;
参考文献
Barder, Tomothy J.; Walton, Richard A.
Inorganic Chemistry, 1982 , vol. 21, p. 2510 - 2511
