2-氨基-4,6-二(2-甲基-2-丙基)苯酚合成路线 (共 21 条)
反应条件
cobalt(II)salen; oxygen in methanol T=25°C; 0.3 h;
参考文献
Chemistry Letters, , # 9 p. 819 - 820
反应条件
1: With ammonium hydroxide in methanol
T=20°C; 0.166667 h;
2: With sodium tetrahydroborate
参考文献
Lodyato, Vladimir I.; Yurkova, Irina L.; Sorokin, Viktor L.; Shadyro, Oleg I.; Dolgopalets, Vladimir I.; Kisel, Mikhail A.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 6 p. 1179 - 1182
反应条件
1 Pd/C; hydrogen in methanol
参考文献
Evangelio, Emi; Saiz-Poseu, Javier; Maspoch, Daniel; Wurst, Klaus; Busque, Felix; Ruiz-Molina, Daniel
European Journal of Inorganic Chemistry, 2008 , # 14 p. 2278 - 2285
反应条件
1: With nitric acid
2: With hydrogen; palladium on activated charcoal in ethanol
参考文献
Fu, Yu-Qin; Li, Zai-Chun; Ding, Li-Na; Tao, Jing-Chao; Zhang, Sheng-Hong; Tang, Ming-Sheng
Tetrahedron Asymmetry, 2006 , vol. 17, # 24 p. 3351 - 3357
参考文献
Vertex Pharmaceuticals Incorported
Patent: US2011/98311 A1, 2011 ;
反应条件
in ethanol; water
T=50°C; 5 h;
参考文献
Vinsova, Jarmila; Horak, Vaclav; Buchta, Vladimir; Kaustova, Jarmila
Molecules, 2005 , vol. 10, # 3 p. 760 - 770
反应条件
in toluene
2 h; Heating;
参考文献
Fukata, Gouki; Sakamoto, Naoya; Tashiro, Massashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 12 p. 2841 - 2848
反应条件
in ethanol; water
T=50°C; 5 h;
参考文献
Vinsova, Jarmila; Horak, Vaclav; Buchta, Vladimir; Kaustova, Jarmila
Molecules, 2005 , vol. 10, # 3 p. 760 - 770
反应条件
hydrogenchloride; zinc in ethanol
Heating; Yield given;
参考文献
Ivakhnenko, E. P.; Lyubchenko, S. N.; Kogan, V. A.; Olekhnovich, L. P.; Prokof'ev, A. I.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 4 p. 869 - 872,765 - 768
反应条件
in ethanol; water
T=50°C; 5 h;
参考文献
Vinsova, Jarmila; Horak, Vaclav; Buchta, Vladimir; Kaustova, Jarmila
Molecules, 2005 , vol. 10, # 3 p. 760 - 770