2-全氟丙氧基全氟丙基三氟乙烯基醚合成路线 (共 12 条)
反应条件
sodium carbonate in diethylene glycol dimethyl ether T=20°C; Elimination; 52 h;
参考文献
Journal of Fluorine Chemistry, , vol. 106, # 1 p. 13 - 24
反应条件
potassium fluoride in acetonitrile T=70°C; 4 h; Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=75°C; 15 h;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=75°C; 20 h; Further byproducts given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=70°C; 16 h;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
cesium fluoride in diethyl ether T=0°C; 3 h; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 1 p. 61 - 66
反应条件
1: 75 percent / 2.85M CH3MgBr / diethyl ether; tetrahydrofuran / 5 h / -60 - -50 °C 2: CsF / diethyl ether / 3 h / 0 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 1 p. 61 - 66
反应条件
1: 66 percent / n-C4H9Li / diethyl ether / 24 h / Ambient temperature 2: lithium ethoxide / diethyl ether / 72 h / Ambient temperature View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 18, p. 243 - 258
反应条件
1: With Cu2Cl2 in acetonitrile oligomerization; 2: With sodium carbonate in diethylene glycol dimethyl ether Elimination; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 12 p. 1715 - 1720
反应条件
potassium fluoride in acetonitrile also with CsF; also with Br2 and further substrates; Product distributionMechanism;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100