1-硝基-2-[(三氟甲基)硫代]苯合成路线 （共 15 条）
反应条件
1: aq. N2H4 2: (i) aq. HNO3, NaNO2, (ii) aq. NaNO2, Na2S2O3, CuSO4 View Scheme
参考文献
Yagupol'skii,L.M.; Boiko,V.N.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, # 1 p. 195 - 198,179 - 182
反应条件
(i) aq. HNO3, NaNO2, (ii) aq. NaNO2, Na2S2O3, CuSO4; Multistep reaction;
参考文献
Yagupol'skii,L.M.; Boiko,V.N.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, # 1 p. 195 - 198,179 - 182
反应条件
1: 17 percent / CrO3 / 100 °C 2: 38 percent Chromat. / tetra-n-butylammonium fluoride / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
反应条件
1: 17 percent / CrO3 / 100 °C 2: 100 percent Chromat. / KF, tetraphenylphosphonium bromide / dimethylsulfoxide / 0.25 h / 130 °C / also with tetra-n-butylammonium fluoride (THF, 20 deg C), other aryltrifluoromethyl sulphones as substrates View Scheme
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
反应条件
chromium(VI) oxide
T=100°C;
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
