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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
16451-50-6
合成路线
（共 12 条）
138602-98-9
→
反应条件
16451-50-6
反应条件
hydrogen; palladium on activated charcoal in ethanol P=760 Torr; 10 h; Ambient temperature;
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Kagamihara, Yasuhiro; Tanaka, Sachi; Inoue, Atsushi; Oku, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1412 - 1421
115404-90-5
→
反应条件
16451-50-6
反应条件
hydrogenchloride in methanol 14 h; Ambient temperature;
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Kagamihara, Yasuhiro; Tanaka, Sachi; Inoue, Atsushi; Oku, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1412 - 1421
54876-99-2
→
反应条件
16451-50-6
反应条件
1: 98 percent / trimethylsilyl trifluoromethanesulfonate (TMSOTf) / tetrahydrofuran / 1 h / 25 °C 2: trimethylsilyl trifluoromethanesulfonate (TMSOTf) / CH2Cl2 / 18 h / -40 °C 3: 88 percent / p-toluenesulfonic acid / methanol / Ambient temperature View Scheme
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Kagamihara, Yasuhiro; Tanaka, Sachi; Inoue, Atsushi; Oku, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1412 - 1421
115346-91-3
→
反应条件
16451-50-6
反应条件
1: trimethylsilyl trifluoromethanesulfonate (TMSOTf) / CH2Cl2 / 18 h / -40 °C 2: 88 percent / p-toluenesulfonic acid / methanol / Ambient temperature View Scheme
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Kagamihara, Yasuhiro; Tanaka, Sachi; Inoue, Atsushi; Oku, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1412 - 1421
40309-42-0
3-羟基-4-甲基戊酸乙酯
→
反应条件
16451-50-6
反应条件
1: LiAlH4 / tetrahydrofuran / Heating 2: 98 percent / trimethylsilyl trifluoromethanesulfonate (TMSOTf) / tetrahydrofuran / 1 h / 25 °C 3: trimethylsilyl trifluoromethanesulfonate (TMSOTf) / CH2Cl2 / 18 h / -40 °C 4: 88 percent / p-toluenesulfonic acid / methanol / Ambient temperature View Scheme
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Kagamihara, Yasuhiro; Tanaka, Sachi; Inoue, Atsushi; Oku, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1412 - 1421
65596-31-8
3-羟基-4-甲基戊酸甲酯
→
反应条件
16451-50-6
反应条件
1: With sodium tetrahydroborate in ethanol 2: With lithium aluminium tetrahydride in diethyl ether
参考文献
Van De Waal, Matthijs; Niclass, Yvan; Snowden, Roger L.; Bernardinelli, Geerald; Escher, Sina
Helvetica Chimica Acta, 2002 , vol. 85, # 5 p. 1246 - 1260
42558-54-3
异丁酰醋酸甲酯
→
反应条件
16451-50-6
反应条件
1.1: 28.3 percent / baker's yeast; sucrose / H2O 2.1: NaBH4 / ethanol 2.2: LiAlH4 / diethyl ether View Scheme
参考文献
Van De Waal, Matthijs; Niclass, Yvan; Snowden, Roger L.; Bernardinelli, Geerald; Escher, Sina
Helvetica Chimica Acta, 2002 , vol. 85, # 5 p. 1246 - 1260
63674-22-6
→
反应条件
16451-50-6
反应条件
lithium aluminium tetrahydride in diethyl ether 2 h; Heating;
参考文献
Buechi,G. et al.
Journal of the Chemical Society, 1961 , p. 2843 - 2860
2351-97-5
→
反应条件
16451-50-6
反应条件
1: DIBAL 2: 2.) Red-Al / 1.) Sharpless epoxidation View Scheme
参考文献
Ishiwata, Hiroyuki; Sone, Hiroki; Kigoshi, Hideo; Yamada, Kiyoyuki
Tetrahedron, 1994 , vol. 50, # 45 p. 12853 - 12882
5362-55-0
→
反应条件
16451-50-6
+
16451-48-2
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride 1.) Sharpless epoxidation; Multistep reaction. Title compound not separated from byproducts;
参考文献
Ishiwata, Hiroyuki; Sone, Hiroki; Kigoshi, Hideo; Yamada, Kiyoyuki
Tetrahedron, 1994 , vol. 50, # 45 p. 12853 - 12882
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