2-((4-甲基苯基)硫代)-苯胺合成路线 （共 13 条）
反应条件
sodium tetrahydroborate; 1,10-phenanthroline; CuSO4‵5H2O in ethanol T=20°C; 8 h;
参考文献
Kumar, Amit; Kumar, Sangit
Tetrahedron, 2014 , vol. 70, # 9 p. 1763 - 1772
反应条件
hydrogen; nickel in ethanol T=60°C; P=77572.2 Torr; 4 h;
参考文献
Bethegnies; Marcincal-Lefebvre; Brunet; Cazin; Damas
Farmaco, 1989 , vol. 44, # 7-8 p. 683 - 694
反应条件
tetra(n-butyl)ammonium hydroxide; water; copper(l) chloride T=50°C; 12 h; Inert atmosphere;
参考文献
Feng, Yi-Si; Qi, Hong-Xia; Wang, Wei-Cheng; Liang, Yu-Feng; Xu, Hua-Jian
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2914 - 2917
反应条件
2,2'-bi-1H-imidazole; copper (II) acetate monohydrate; caesium carbonate in dimethyl sulfoxide T=80°C; Ullmann Condensation; 3 h; Schlenk techniqueInert atmosphere; chemoselective reaction;
参考文献
Zong, Chenglong; Liu, Jianli; Chen, Shengyan; Zeng, Runsheng; Zou, Jianping
Chinese Journal of Chemistry, 2014 , vol. 32, # 3 p. 212 - 218
反应条件
1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature 2: 76 percent / hydrogen / Ni / ethanol / 4 h / 60 °C / 77572.2 Torr View Scheme
参考文献
Gilman; Broadbent
Journal of the American Chemical Society, 1947 , vol. 69, p. 2053,2055
反应条件
1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature 2: 76 percent / hydrogen / Ni / ethanol / 4 h / 60 °C / 77572.2 Torr View Scheme
参考文献
Bethegnies; Marcincal-Lefebvre; Brunet; Cazin; Damas
Farmaco, 1989 , vol. 44, # 7-8 p. 683 - 694
反应条件
1: ethanol 2: Raney nickel; ethanol / Hydrogenation View Scheme
参考文献
Gilman; Broadbent
Journal of the American Chemical Society, 1947 , vol. 69, p. 2053,2055
反应条件
T=750°C; P=0.001 Torr; 0.25 h;
参考文献
Cadogan, J. I. G.; Hickson, Clare L.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 377 - 384
反应条件
T=750°C; P=0.001 Torr; 0.25 h; or the 4'-methyl derivative; Mechanism;
参考文献
Cadogan, J. I. G.; Hickson, Clare L.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 377 - 384
反应条件
tert-Butyl thionitrate
T=160°C; 0.5 h;
参考文献
Oae, Shigeru; Iida, Kazuyuki; Shinhama, Koichi; Takata, Toshikazu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 8 p. 2374 - 2378
