4,4,4,-三氟丁烷-1-醇甲烷硫酸盐合成路线 (共 3 条)
反应条件
pyridine in dichloromethane T=0 - 20°C; 2 h;
参考文献
MERCK SHARP and DOHME LIMITED; MERCK and CO., INC.
Patent: WO2007/125364 A1, 2007 ;
Location in patent: Page/Page column 32 ;
WO 2007/125364 A1
反应条件
triethylamine in dichloromethane; water
参考文献
Synthelabo
Patent: US5525619 A1, 1996 ;
反应条件
in dimethyl sulfoxide
T=60°C; 2 h;
参考文献
MERCK SHARP and DOHME LIMITED; MERCK and CO., INC.
Patent: WO2007/125364 A1, 2007 ;
Location in patent: Page/Page column 32 ;
WO 2007/125364 A1