反应条件
1: 56 percent / LiI / pyridine / 16 h / 130 °C 2: 1.) EDS, DMAP, DMAP*HCl, 2.) i-Pr2NEt, <(2-furyl)3P>2PdCl2 / 1.) CH2Cl2, room temperature, 5 h, 2.) THF, DMF, room temperature, 7 h 3: 90 percent / TBAF, AcOH / tetrahydrofuran / 3 h / 0 °C 4: 71 percent / HF*pyr, pyridine / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Smith III, Amos B.; Condon, Stephen M.; McCauley, John A.; Leazer Jr., Johnnie L.; Leahy, James W.; Maleczka Jr., Robert E.
Journal of the American Chemical Society, 1995 , vol. 117, # 19 p. 5407 - 5408
