反应条件
1: 1.) HMPT, 2.) n-BuLi / 1.) THF, 2.) THF 2: 94 percent / DDQ / CH2Cl2; H2O 3: 86 percent / (CF3CO2)2IPh / methanol; H2O; tetrahydrofuran 4: 1.) Bu3SnH, (Ph3P)2PdCl2, 2.) EDC, DMAP, DMAP*HCl, 3.) <(2-furyl)3P>2PdCl2, DIPEA 5: 1.) TBAF, AcOH, 2.) HF*pyr, pyr / 1.) 0 deg C, 2.) THF, RT View Scheme
参考文献
Smith III, Amos B.; Condon, Stephen M.; McCauley, John A.; Leazer Jr., Johnnie L.; Leahy, James W.; Maleczka Jr., Robert E.
Journal of the American Chemical Society, 1995 , vol. 117, # 19 p. 5407 - 5408
