in neat (no solvent)
heating an excess of PSCl3 with PH4I in a sealing tube at 100 °C;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1896 , vol. 122, p. 1200 - 1202
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Gmelin Handbook: P: MVol.C, 260, page 594 - 596
in neat (no solvent)
heating stepwise in sealed tube at 125 to 135°C and 250 to 260°C;;
参考文献
Fireman, E.; Fireman, P.
American Chemical Journal, 1903 , vol. 30, p. 116 - 133
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Gmelin Handbook: P: MVol.C, 230, page 527 - 529
in neat (no solvent)
adding components separately into sealed tube and heating to 95 to 105°C;;
参考文献
Fireman, E.; Fireman, P.
American Chemical Journal, 1903 , vol. 30, p. 116 - 133
Full Text Show Details
Gmelin Handbook: P: MVol.C, 230, page 527 - 529
