(2-甲基-3-丁烯基)苯合成路线 (共 16 条)
反应条件
copper(I) bromide in tetrahydrofuran
T=-30 - 0°C; 1 h;
参考文献
Gendreau,Y. et al.
Journal of Organometallic Chemistry, 1977 , vol. 142, p. 1 - 7
反应条件
benzophenone
0.25 h; Irradiation; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Creary, Xavier
Journal of the American Chemical Society, 1980 , vol. 102, # 5 p. 1611 - 1618
反应条件
Fe(acetylacetonate)2 in tetrahydrofuran; diethyl ether
T=15°C; 4.5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Zubritskii, L. M.; Romashchenkova, N. D.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2465 - 2477
反应条件
tetrakis(triphenylphosphine) palladium(0); ammonium formate; triphenylphosphine in tetrahydrofuran
T=60°C; 18 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ono, Noboru; Hamamoto, Isami; Kamimura, Akio; Kaji, Aritsune
Journal of Organic Chemistry, 1986 , vol. 51, # 19 p. 3734 - 3736
反应条件
Fe(acetylacetonate)2 in tetrahydrofuran; diethyl ether
T=5 - 15°C; 4.5 h; other temperature; other catalyst; other products; Product distributionMechanism;
参考文献
Zubritskii, L. M.; Romashchenkova, N. D.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2465 - 2477
反应条件
multistep reaction: regioselective protodesilylation; other cyclopropylmethylsilanes;
参考文献
Fleming; Sanderson; Terrett
Synthesis, 1992 , # 1-2 p. 69 - 74