3,3-二甲基-1-溴丁烷 [1647-23-0]合成路线 （共 26 条）
反应条件
pyridine; phosphorus tribromide Bromination; 12 h; Heating;
参考文献
Hamano, Hiroshi; Nagata, Keiichi; Fukada, Nobuo; Shimotahira, Hiroshi; Ju, Xiu-Lian; Ozoe, Yoshihisa
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 3 p. 665 - 674
参考文献
Chem. Zentralbl., , vol. 77, # I p. 1233
反应条件
iron(III) chloride T=30°C; unter Druck;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 1153
US2434289 , ;
参考文献
Journal of Organic Chemistry, , vol. 38, p. 1367 - 1369
反应条件
in dichloromethane-d2 (N2), NMR-tube, cooled to -80°C, kept at -40°C for 12 h; H-, P-NMR, GLC;
参考文献
Organometallics, , vol. 10, p. 2327 - 2334
反应条件
1: 72.1 percent / LiAlH4 / tetrahydrofuran 2: 37.4 percent / PBr3 / diethyl ether; diethyl ether / 16 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 9 p. 2391 - 2398
反应条件
1: PCl5 2: sodium; water 3: HBr View Scheme
参考文献
Chem. Zentralbl., , vol. 77, # I p. 1233
反应条件
1: ethanolic KOH / 150 °C 2: sodium; water 3: HBr View Scheme
参考文献
Chem. Zentralbl., , vol. 77, # I p. 1233
反应条件
1: sodium; water 2: HBr View Scheme
参考文献
Chem. Zentralbl., , vol. 77, # I p. 1233
反应条件
organoaluminiumhydride; water; bromine 2) -40 to 20 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 4 p. 934 - 935,829 - 830
