3,3-二甲基-1-溴丁烷 [1647-23-0]合成路线 （共 26 条）
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3592
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3592
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3592
参考文献
Chem. Zentralbl., , vol. 77, # II p. 1233
参考文献
Universal Oil Prod.Co.
Patent: US2434289 , 1944 ;
参考文献
Universal Oil Prod.Co.
Patent: US2434289 , 1944 ;
反应条件
1: potassium acetate / und man verseift das erhaltene Acetat durch Erhitzen mit gepulvertem Kali auf 200grad View Scheme
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # I p. 1233
反应条件
1.1: Mg / diethyl ether / 2 h / 20 °C 1.2: 43.9 percent / diethyl ether / 1 h / 20 °C 2.1: 44.8 percent / LiAlH4 / diethyl ether / 5 h / Heating View Scheme
参考文献
Hamano, Hiroshi; Nagata, Keiichi; Fukada, Nobuo; Shimotahira, Hiroshi; Ju, Xiu-Lian; Ozoe, Yoshihisa
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 3 p. 665 - 674
反应条件
1: 1-bromo-3,3-dimethylbutane With magnesium in diethyl ether T=20°C; Grignard reaction; 2 h; 2: carbon dioxide in diethyl ether T=20°C; Carboxylation; 1 h;
参考文献
Hamano, Hiroshi; Nagata, Keiichi; Fukada, Nobuo; Shimotahira, Hiroshi; Ju, Xiu-Lian; Ozoe, Yoshihisa
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 3 p. 665 - 674
反应条件
potassium acetate und man verseift das erhaltene Acetat durch Erhitzen mit gepulvertem Kali auf 200grad;
参考文献
Banthorpe,D.V. et al.
Journal of the Chemical Society, 1960 , p. 4054 - 4087
