1,4-二[[4-(2-羟基乙氧基)苯基]氨基]蒽醌合成路线 （共 5 条）
反应条件
sodium hydroxide in ethylene glycol dimethyl ether 4 h; Reflux;
参考文献
Dollendorf, Christian; Kreth, Susanne Katharina; Choi, Soo Whan; Ritter, Helmut
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 453 - 459
反应条件
1: disodium hydrogenphosphate / 1-methyl-pyrrolidin-2-one / 15 h / 150 - 180 °C / |Inert atmosphere 2: sodium hydroxide / ethylene glycol dimethyl ether / 4 h / |Reflux View Scheme
参考文献
Dollendorf, Christian; Kreth, Susanne Katharina; Choi, Soo Whan; Ritter, Helmut
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 453 - 459
反应条件
1: disodium hydrogenphosphate / 1-methyl-pyrrolidin-2-one / 15 h / 150 - 180 °C / |Inert atmosphere 2: sodium hydroxide / ethylene glycol dimethyl ether / 4 h / |Reflux View Scheme
参考文献
Dollendorf, Christian; Kreth, Susanne Katharina; Choi, Soo Whan; Ritter, Helmut
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 453 - 459
反应条件
1: sulfuric acid / 4 h / 150 °C 2: disodium hydrogenphosphate / 1-methyl-pyrrolidin-2-one / 15 h / 150 - 180 °C / |Inert atmosphere 3: sodium hydroxide / ethylene glycol dimethyl ether / 4 h / |Reflux View Scheme
参考文献
Dollendorf, Christian; Kreth, Susanne Katharina; Choi, Soo Whan; Ritter, Helmut
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 453 - 459
反应条件
1: phthalic anhydride; AlCl3, aluminium chloride; sodium chloride / 6 h / 115 °C 2: sulfuric acid / 4 h / 150 °C 3: disodium hydrogenphosphate / 1-methyl-pyrrolidin-2-one / 15 h / 150 - 180 °C / |Inert atmosphere 4: sodium hydroxide / ethylene glycol dimethyl ether / 4 h / |Reflux View Scheme
参考文献
Dollendorf, Christian; Kreth, Susanne Katharina; Choi, Soo Whan; Ritter, Helmut
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 453 - 459
