2,3-二苯基-2H-氮丙啶合成路线 （共 24 条）
反应条件
sodium hydride in N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
Okamoto, Kazuhiro; Mashida, Ayano; Watanabe, Masahito; Ohe, Kouichi
Chemical Communications, 2012 , vol. 48, # 29 p. 3554 - 3556
反应条件
lithium azide in acetonitrile 20 h; Ambient temperature; Further byproducts given;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
lithium azide in acetonitrile 20 h; Ambient temperature; Further byproducts given;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
lithium azide in acetonitrile 20 h; Ambient temperature; Further byproducts given;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
3.5 h; microwave irradiation;
参考文献
Singh, Pradeep N. D.; Carter, Carrie L.; Gudmundsdottir, Anna D.
Tetrahedron Letters, 2003 , vol. 44, # 35 p. 6763 - 6765
反应条件
1: trifluoroacetic acid / benzene / 4 h / Reflux 2: 13 h / 40 °C 3: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C View Scheme
参考文献
Loy, Nicole S. Y.; Singh, Alok; Xu, Xianxiu; Park, Cheol-Min
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2212 - 2216
Angew. Chem., vol. 125, # 8 p. 2268 - 2272,5
反应条件
1: 13 h / 40 °C 2: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C View Scheme
参考文献
Loy, Nicole S. Y.; Singh, Alok; Xu, Xianxiu; Park, Cheol-Min
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2212 - 2216
Angew. Chem., vol. 125, # 8 p. 2268 - 2272,5
反应条件
1: 84 percent / Na-azide, iodine monochloride / acetonitrile / -40 to -30 deg C, 30 min; to RT, 20 h 2: 93 percent / t-BuOK / diethyl ether / 8 h / -5 - 0 °C 3: petroleum ether / 1.25 h / Heating View Scheme
参考文献
Perrocheau, Jacques; Danion-Bougot, Renee; Carrie, Robert
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 973 - 985
反应条件
lithium azide in acetonitrile 20 h; Ambient temperature;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
T=240 - 250°C; 0.75 h; other 1-aroylamino-4,5-diaryl-1,2,3-triazoles; MechanismProduct distribution;
参考文献
Hadjiantoniou-Maroulis; Charalambopoulos; Maroulis
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 4 p. 891 - 894
