2,5-二碘-3-甲基噻吩合成路线 (共 3 条)
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate; zinc(II) chloride in acetic acid 4 h; Ambient temperature;
参考文献
Okamoto, Tsuyoshi; Kakinami, Takaaki; Fujimoto, Hiroshi; Kajigaeshi, Shoji
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2566 - 2568
反应条件
NH4I; dihydrogen peroxide in water; acetic acid 20 h; Green chemistry; regioselective reaction;
参考文献
D'Aleo, Danielle N.; Allard, Sheena R.; Foglia, Cassandra C.; Parent, Shawna L.M.; Rohr, David J.; Gottardo, Christine; MacKinnon, Craig D.
Canadian Journal of Chemistry, 2013 , vol. 91, # 8 p. 679 - 683
反应条件
copper(II) oxide in methanol
96 h; Heating;
参考文献
Hallberg, Anders; Frejd, Torbjoern; Gronowitz, Salo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1390 - 1392