4-(5-溴噻吩-2-基)吡啶合成路线 (共 4 条)
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide Bromination; 25.5 h;
参考文献
Effenberger; Endtner; Miehlich; Munter; Vollmer
Synthesis, 2000 , # 9 p. 1229 - 1236
反应条件
1: 90 percent / aq. Na2CO3 / Pd(PPh3)4 / 1,2-dimethoxy-ethane / Heating 2: 84 percent / NBS / dimethylformamide / 25.5 h View Scheme
参考文献
Abbotto, Alessandro; Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5755 - 5765
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; toluene / Reflux 2: bromine / dichloromethane / 0.42 h / 20 °C View Scheme
参考文献
Sahu, Duryodhan; Padhy, Harihara; Patra, Dhananjaya; Kekuda, Dhananjay; Chu, Chih-Wei; Chiang, I.-Hung; Lin, Hong-Cheu
Polymer, 2010 , vol. 51, # 26 p. 6182 - 6192
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether Ambient temperature;
参考文献
Abbotto, Alessandro; Bradamante, Silvia; Facchetti, Antonio; Pagani, Giorgio A.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5755 - 5765