(S)-(+)-1-苄氧基-3-(对甲苯磺酰氧基)-2-丙醇合成路线 （共 12 条）
反应条件
3 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane 1.) O deg C, 12 h; 2.) 20 deg C, 2 h;
参考文献
Byun, Hoe-Sup; Bittman, Robert
Tetrahedron Letters, 1989 , vol. 30, # 21 p. 2751 - 2754
反应条件
pyridine 0 deg C, 0.5 h; r.t., 18 h;
参考文献
Baig, Mirza Hamed A.; Baskaran, Subramanian; Banerjee, Sharmila; Trivedi, Girish K.
Tetrahedron, 1995 , vol. 51, # 16 p. 4723 - 4732
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 130, # 2 p. 412 - 413
反应条件
boron trifluoride diethyl etherate in dichloromethane T=4°C; 18 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 3077 - 3079
反应条件
boron trifluoride diethyl etherate in dichloromethane T=4°C; 18 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 3077 - 3079
反应条件
1: 91 percent / 1N H2SO4 / 1 h / 90 °C 2: 64.5 percent / pyridine / CHCl3 / Ambient temperature View Scheme
参考文献
Helvetica Chimica Acta, , vol. 65, # 3 p. 1059 - 1084
反应条件
1: 94 percent / 30percent NaOH / tributylbenzylammonium chloride / 4 h / 50 °C 2: 91 percent / 1N H2SO4 / 1 h / 90 °C 3: 64.5 percent / pyridine / CHCl3 / Ambient temperature View Scheme
参考文献
Helvetica Chimica Acta, , vol. 65, # 3 p. 1059 - 1084
反应条件
1: NaNO2, H2SO4 / 16 h / Ambient temperature 2: 70 percent / H+ 3: LiAlH4 / tetrahydrofuran 4: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: 70 percent / H+ 2: LiAlH4 / tetrahydrofuran 3: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: LiAlH4 / tetrahydrofuran 2: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
