反应条件
1: N,N'-dimethyl-N,N'-propyleneurea; lithium diisopropyl amide / tetrahydrofuran / -40 - 0 °C / |Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / |Inert atmosphere
3: 1-methyl-1H-imidazole / tetrahydrofuran / 0 °C / |Inert atmosphere
4: 1,10-phenanthroline; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / |Inert atmosphere
View Scheme
参考文献
Perry, Matthew A.; Hill, Richard R.; Rychnovsky, Scott D.
Organic Letters, 2013 , vol. 15, # 9 p. 2226 - 2229