4-甲基-4-硝基戊酸甲酯合成路线 （共 14 条）
反应条件
Merrifield resin-bound azidoproazaphosphatrane in tetrahydrofuran T=20°C; Michael addition; 10 h;
参考文献
Venkat Reddy, Chinta Reddy; Verkade, John G.
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 3093 - 3096
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
参考文献
Wang, Wengui; Yu, Marvin
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7141 - 7143
反应条件
sodium tetrahydroborate in methanol 24 h; Ambient temperature;
参考文献
Ho, Tse-Lok
Synthetic Communications, 1982 , vol. 12, # 5 p. 339 - 342
参考文献
Bulletin of the Chemical Society of Japan, , vol. 49, p. 3181 - 3184
反应条件
sodium hydride in dimethyl sulfoxide SRN1 reaction under various conditions (with/without light, oxygene, galvinoxyde); Product distributionMechanism;
参考文献
Tetrahedron Letters, , vol. 25, # 22 p. 2347 - 2350
反应条件
(i) H2, Raney-Ni, (ii) aq. HCl; Multistep reaction;
参考文献
Kaji,E. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 3181 - 3184
反应条件
sodium tetrahydroborate; 0.5NiCl2*6H2O in methanol T=0 - 25°C; 48 h;
参考文献
Coyle, Jason P.; Kurek, Agnieszka; Pallister, Peter J.; Sirianni, Eric R.; Yap, Glenn P. A.; Barry, Sean T.
Chemical Communications, 2012 , vol. 48, # 84 p. 10440 - 10442
反应条件
1: Raney nickel; ethanol / 60 °C / 51485.6 Torr 2: lithium alanate; tetrahydrofuran View Scheme
参考文献
Moffett; White
Journal of Organic Chemistry, 1952 , vol. 17, p. 407,412
反应条件
1: With sodium hydroxide; ethanol; water 24 h; 2: With hydrogenchloride
参考文献
SANWA KAGAKU KENKYUSHO CO., LTD.
Patent: EP1595866 A1, 2005 ;
Location in patent: Page/Page column 12 ;
反应条件
1: Raney nickel; ethanol / 60 °C / 51485.6 Torr
2: lithium alanate; tetrahydrofuran
3: 160 °C
View Scheme
参考文献
Moffett; White
Journal of Organic Chemistry, 1952 , vol. 17, p. 407,412
