1-环丙基甲基-4-甲氧基-苯合成路线 （共 10 条）
反应条件
copper(l) iodide in tetrahydrofuran T=70°C; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
sodium in methanol; diethyl ether 3 h;
参考文献
Mochalov; Gazzaeva; Fedotov; Trofimova; Trushkov; Zefirov
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 8 p. 1098 - 1112
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C 1.2: 8 h / 20 °C 2.1: triethylsilane; anhydrous iron chloride / dichloromethane / 1.5 h / 20 °C View Scheme
参考文献
Fan, Xiaohui; Cui, Xiao-Meng; Guan, Yong-Hong; Fu, Lin-An; Lv, Hao; Guo, Kun; Zhu, Hong-Bo
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 498 - 501
反应条件
1: 66 percent / Et3BnNCl; aq. NaOH / 3 h 2: 71 percent / sodium / diethyl ether; methanol / 3 h View Scheme
参考文献
Mochalov; Gazzaeva; Fedotov; Trofimova; Trushkov; Zefirov
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 8 p. 1098 - 1112
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h 1.2: 2 h 2.1: copper(l) iodide / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere View Scheme
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
1.1: triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h 2.2: 2 h 3.1: copper(l) iodide / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere View Scheme
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
sodium hydride 1.) glyme, ethanol, 6 h, 70 deg C, 2.) 12 h, 80 deg C; Yield given. Multistep reaction;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
nitric acid in acetic anhydride T=-50°C; 1 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 3 p. 406 - 416
反应条件
nitric acid in acetic anhydride T=-50°C; 1 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 3 p. 406 - 416
反应条件
4-nitro-benzoic acid in dichloromethane
1.) 1 h, room temp., 2.) 1 h, reflux;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
