反应条件
1.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 - 20 °C / |Inert atmosphere
1.2: 24 h / 20 °C / |Inert atmosphere
2.1: N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine / N,N-dimethyl-formamide / 72 h / |Inert atmosphere; |Glovebox; |UV-irradiation
View Scheme
参考文献
Doni, Eswararao; O'Sullivan, Steven; Murphy, John A.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2239 - 2242
Angew. Chem., 2013 , vol. 125, # 8 p. 2295 - 2298,4
