in decane addn. of a soln. of Me3SiNHMe in decane to 2,4,6-tri-t-butylphenyl difluoroborane and vigorously refluxing for 3-5 d under N2; distilling off the excess of amine and subliming the methylaminoborane from the residue under vacuum, elem. anal.;
参考文献
Geschwentner, M.; Elter, G.; Meller, A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1993 , vol. 619, p. 1474 - 1478
