2-[(4-甲基苯基)氨基]苯甲酸合成路线 （共 21 条）
参考文献
Hoechster Farbw.
Patent: DE145189 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 7, p. 122
反应条件
Yield given. Multistep reaction;
参考文献
Tomosaka, Hideyuki; Omata, Saburo; Hasegawa, Eietsu; Anzai, Kentaro
Bioscience, Biotechnology and Biochemistry, 1997 , vol. 61, # 7 p. 1121 - 1125
参考文献
Ullmann
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 325
参考文献
Dirscherl; Thron
Justus Liebigs Annalen der Chemie, 1933 , vol. 504, p. 297,302
反应条件
xylene; trichlorophosphate
参考文献
Drosdow
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1641,1643
Chem. Zentralbl., 1937 , vol. 108, # I p. 2603
参考文献
Nadaraj; Kalaivani; Selvi, S. Thamarai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 8 p. 1958 - 1960
反应条件
xylene; trichlorophosphate
参考文献
Drosdow
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1641,1643
Chem. Zentralbl., 1937 , vol. 108, # I p. 2603
反应条件
sulfuric acid
T=100°C; Microwave irradiation; Kinetics; Temperature;
参考文献
Markovich; Kudryavtseva; Brylev; Koroleva
Russian Journal of General Chemistry, 2012 , vol. 82, # 1 p. 149 - 152
反应条件
1: phosphoryl chloride; xylene
View Scheme
参考文献
Drosdow
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1641,1643
Chem. Zentralbl., 1937 , vol. 108, # I p. 2603
反应条件
1: 72 percent / sulfuric acid / 6 h / Heating
2: 66 percent / hydrazine hydrate / 12 h / 180 - 190 °C
3: 93 percent / pyridine / 2 h / Ambient temperature
4: 62 percent / anhyd. sodium carbonate / ethane-1,2-diol / 0.02 h / 170 °C
5: 83 percent / trifluoroacetic acid / 30 h / Ambient temperature
View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 839 - 853
