反应条件
1: 78 percent / potassium t-butoxide, KI / 2-methyl-propan-2-ol / 1.) room temp., 1-2 h; 2.) reflux, 22-24 h
2: 65 percent / KOH / aq. ethanol / 12 h / Heating
3: 1.) Hg(OAc)2; 2.) NaBH4, aq. NaOH / 1.) H2O, THF, room temp., 10 min; 2.) 10 min, ice/water bath
4: 65 percent / n-butyl nitrite, aq. HCl / aq. ethanol / 6 h
View Scheme
参考文献
Mahajan, Jaswant Rai; Araujo, Hugo Clemente de
Synthesis, 1981 , # 1 p. 49 - 51
