2-羟基-3-硝基-4-氯吡啶合成路线 (共 12 条)
反应条件
1: With lithium chloride; trichlorophosphate T=105°C; 2.5 h; Industrial scale; 2: With hydrogenchloride T=105°C; 1 h; Industrial scale;
参考文献
Cleator, Ed; Scott, Jeremy P.; Avalle, Paulo; Bio, Matthew M.; Brewer, Sarah E.; Davies, Antony J.; Gibb, Andrew D.; Sheen, Faye J.; Stewart, Gavin W.; Wallace, Debra J.; Wilson., Robert D.
Organic Process Research and Development, 2013 , vol. 17, # 12 p. 1561 - 1567
反应条件
in tetrahydrofuran
T=140°C; P=12929 Torr; 0.0833333 h; Irradiation;
参考文献
Hergenrother, Paul J.; Putt, Karson S.; Liu, Xianjun
Patent: US2007/32496 A1, 2007 ;
Location in patent: Page/Page column Sheet 23; 5; 27 ;