4,4'-亚乙基二苯甲醚合成路线 (共 130 条)
反应条件
Raney-Nickel W-2A in ethanol
Heating;
参考文献
Latif, K. A.; Ali, M. Umar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 471 - 473
反应条件
naphthalenyllithium; methyl iodide
1.) Et2O-THF-light petroleum, -95 degC, 45 min, 2.) -95 deg C, 20 min; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Smith, Keith; Hou, Daunjie
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , p. 185 - 186
反应条件
Irradiation; Product distributionKinetics;
参考文献
Johnston, Linda J.; Mayo, Paul de; Wong, S. King
Journal of the American Chemical Society, 1982 , vol. 104, # 1 p. 307 - 309
反应条件
iodine; magnesium
1.) ether, reflux, 20 min, 2.) r.t., 5 h; Yield given. Multistep reaction;
参考文献
Tacke; Bentlage-Felten; Linoh; Magda
1986 , vol. 41, # 5 p. 649 - 654
反应条件
naphthalenyllithium
1.) Et2O-THF-light petroleum, -95 degC, 45 min, 2.) -95 deg C, 20 min; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Smith, Keith; Hou, Daunjie
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , p. 185 - 186
反应条件
in acetonitrile
0.05 h; Irradiation;
参考文献
Homma; Yamada
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 7 p. 1198 - 1201
反应条件
Titanium(IV) oxide; silver sulphate
Irradiation;
参考文献
Cermenati, Laura; Fagnoni, Maurizio; Albini, Angelo
Canadian Journal of Chemistry, 2003 , vol. 81, # 6 p. 560 - 566
反应条件
lithium
1. THF, -30 deg C, 2.) THF, 20 deg C, 30 min; Multistep reaction;
参考文献
Muellen, Klaus; Alexander, Juergen; Klabunde, Kay-Uwe; Klaerner, Frank-Gerrit; Lund, Henning; Lund, Torben
Chemische Berichte, 1992 , vol. 125, # 2 p. 505 - 514
反应条件
cesium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
75 h; Ambient temperatureother solvent; Product distribution;
参考文献
Okazaki, Seiji; Shirai, Naohiro; Sato, Yoshiro
Journal of Organic Chemistry, 1990 , vol. 55, # 1 p. 334 - 337
反应条件
silica gel
T=20°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Frederick, Bradley; Johnston, Linda J.; Mayo, Paul de; Wong, S. King
Canadian Journal of Chemistry, 1984 , vol. 62, p. 403 - 410