4,4'-亚乙基二苯甲醚合成路线 （共 130 条）
反应条件
in various solvent(s)
T=23.84°C; Kinetics;
参考文献
Sobek; Martschke; Fischer
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2849 - 2857
反应条件
1: 74 percent / NaOH / H2O / 3 h / Heating
2: 13 percent Chromat. / pentane / 37 °C / Irradiation
View Scheme
参考文献
Bastien, Gerard; Surzur, Jean-Marie
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 1-2 p. 84 - 88
反应条件
1: ozone / dichloromethane / -78 °C
2: 2,4,6-trimethyl-pyridine; manganese; bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane / tetrahydrofuran / 3 h / Inert atmosphere
View Scheme
参考文献
Rosales, Antonio; Munoz-Bascon, Juan; Lopez-Sanchez, Cristobal; Alvarez-Corral, Miriam; Munoz-Dorado, Manuel; Rodriguez-Garcia, Ignacio; Oltra, J. Enrique
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 4171 - 4176
反应条件
1: Grubb's 2nd generation catalyst / dichloromethane / 2 h / 40 °C
2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 6 h / 20 °C
View Scheme
参考文献
Yamaguchi, Yusuke; Okada, Yohei; Chiba, Kazuhiro
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2626 - 2638
参考文献
Fuson; House
Journal of the American Chemical Society, 1953 , vol. 75, p. 1327
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran
22 h; Heating; Title compound not separated from byproducts;
参考文献
Dang, Y.; Geise, H. J.
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 5 p. 375 - 380
反应条件
silica gel
T=-55°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Frederick, Bradley; Johnston, Linda J.; Mayo, Paul de; Wong, S. King
Canadian Journal of Chemistry, 1984 , vol. 62, p. 403 - 410
反应条件
magnesium; copper(l) iodide
1.) ether, 3.5 h, reflux, 2.) THF, -10 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nasipuri, Dhanonjoy; Samaddar, Ashis K.; Das, Gautam
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 9 p. 727 - 734
反应条件
in 1,4-dioxane
Irradiation;
参考文献
Givens,R.S.; Oettle,W.F.
Journal of Organic Chemistry, 1972 , vol. 37, # 26 p. 4325 - 4334
反应条件
1: ozone / dichloromethane / -78 °C
2: manganese; bis(cyclopentadienyl)titanium dichloride / tetrahydrofuran / 0.5 h / Inert atmosphere
View Scheme
参考文献
Rosales, Antonio; Munoz-Bascon, Juan; Lopez-Sanchez, Cristobal; Alvarez-Corral, Miriam; Munoz-Dorado, Manuel; Rodriguez-Garcia, Ignacio; Oltra, J. Enrique
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 4171 - 4176
