1,2,3,4,5,6,7,8-八氢吖啶合成路线 （共 44 条）
反应条件
1: 69 percent / POCl3 / CH2Cl2 / 3 h / 0 - 15 °C 2: 51 percent / POCl3 / 1,2-dichloro-ethane / 4 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 3 p. 922 - 925
反应条件
hydrogen; palladium/alumina in decalin T=150 - 250°C; P=15200 - 53200 Torr; Kinetics;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1769 - 1774
反应条件
hydrogen; palladium/alumina in decalin T=250°C; P=15200 Torr; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1769 - 1774
反应条件
hydrogen; Pt/Al2O3 in decalin T=149.9°C; P=52504.2 Torr; 0.166667 h; effect of time; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3994 - 4001
反应条件
1: 80 percent / sodium azide / dimethylsulfoxide / 1.) 10 deg C, 1 h, 2.) room temperature, 4 h 2: 85 percent / toluene / 2 h / Ambient temperature 3: 80 percent / 1,2,3,4-tetrahydro-naphthalene / 24 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 18, # 13 p. 1475 - 1482
反应条件
nickel; decalin T=150°C; Hydrogenation.unter Druck;
参考文献
Chemische Berichte, , vol. 56, p. 1348
参考文献
Nippon Kagaku Zasshi, , vol. 77, p. 1766,1768
Chem.Abstr., , p. 5234
反应条件
hydroxylamine hydrochloride in isopropyl alcohol Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 20, # 12 p. 1361 - 1364
Khimiya Geterotsiklicheskikh Soedinenii, , # 12 p. 1652 - 1655
反应条件
ammonia; hydrogen; Raney NI/Ru
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 23, # 12 p. 1324 - 1329
Khimiya Geterotsiklicheskikh Soedinenii, , # 12 p. 1645 - 1650
反应条件
in water 2 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 1 p. 38 - 44
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 1 p. 46 - 52
