反应条件
1.1: Inert atmosphere 2.1: [Ni0(1,5-cyclooctadiene)2]; sodium t-butanolate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere 3.1: N-iodo-succinimide; trifluoroacetic acid / 14 h / 23 °C / Inert atmosphere 3.2: 23 °C 4.1: trans-1,2-cyclohexanediamine; potassium carbonate; copper(l) chloride / 1,4-dioxane / 15 h / 110 °C / Inert atmosphere; Darkness 5.1: 7 h / 23 °C 5.2: 23 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 9 p. 2171 - 2173
