N-{(4-氟苯基)[(4-甲基苯基)磺酰基]甲基}甲酰胺合成路线 (共 6 条)
反应条件
chloro-trimethyl-silane in toluene; acetonitrile T=50°C; 5 h;
参考文献
Sisko, Joseph; Mellinger, Mark; Sheldrake, Peter W.; Baine, Neil H.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8113 - 8116
反应条件
formamide in methanol
参考文献
SmithKline Beecham Corporation
Patent: US5739143 A1, 1998 ;
反应条件
1: TMSCl / toluene; acetonitrile / 5 h / 50 °C 2: toluene; acetonitrile / 5 h / 50 °C View Scheme
参考文献
Sisko, Joseph; Mellinger, Mark; Sheldrake, Peter W.; Baine, Neil H.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8113 - 8116
反应条件
in toluene; acetonitrile T=50°C; 5 h;
参考文献
Sisko, Joseph; Mellinger, Mark; Sheldrake, Peter W.; Baine, Neil H.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8113 - 8116
参考文献
SmithKline Beecham Corporation
Patent: US6335340 B1, 2002 ;
Location in patent: Example 23 ;
反应条件
triethylamine; trichlorophosphate in ethylene glycol dimethyl ether
参考文献
SmithKline Beecham Corporation
Patent: US5716955 A1, 1998 ;