1-乙基-1H-苯并三唑合成路线 （共 27 条）
反应条件
potassium hydroxide; PEG-400-Et2 in water; benzene
T=30°C; 3 h;
参考文献
Sukata, Kazuaki
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 280 - 284
反应条件
triethylamine in dichloromethane
T=0 - 5°C; Alkylation; 1 h;
参考文献
Singh, Neera; Dureja, Prem
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997 , vol. 36, # 8 p. 700 - 702
反应条件
sodium hydride in dimethyl sulfoxide
T=20°C; stereoselective reaction;
参考文献
Xiao, Xiaohui; Lin, Daqin; Tong, Shuitian; Luo, Hong; He, Yinfeng; Mo, Hailan
Synlett, 2011 , # 12 p. 1731 - 1734
反应条件
1: toluene / 0.75 h / Heating
2: SOCl2 / toluene / 2 h / Heating
3: 40 percent / methanol / 1 h / Heating
4: toluene; diethyl ether / Heating
View Scheme
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
反应条件
sodium hydroxide
T=110°C; 4 h;
参考文献
Sanna, Paolo; Carta, Antonio; Paglietti, Giuseppe; Bacchi, Alessia; Pelizzi, Giancarlo
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 1 p. 97 - 106
反应条件
in various solvent(s)
20 h; Heating;
参考文献
Katritzky, Alan R.; Belyakov, Sergei A.; Rachwal, Bogumila; Moutou, Jean-Luc
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 700 - 705
反应条件
T=120°C; Title compound not separated from byproducts;
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
1: SOCl2 / toluene / 2 h / Heating
2: 40 percent / methanol / 1 h / Heating
3: toluene; diethyl ether / Heating
View Scheme
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
反应条件
tetraethylammonium iodide in toluene; benzene
48 h; Heating;
参考文献
Katritzky; Wu
Synthesis, 1994 , # 6 p. 597 - 600
反应条件
1: 40 percent / methanol / 1 h / Heating
2: toluene; diethyl ether / Heating
View Scheme
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
