1-乙基-1H-苯并三唑合成路线 (共 27 条)
反应条件
in diethyl ether
1 h; Ambient temperature;
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Caster, Kenneth C.; Mahni, Fatma; Law, Kam Wah; Rubio, Olga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 781 - 790
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 4 h, 2.) THF, hexane, up to 25 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Wu, Jing; Kuzmierkiewicz, Wojciech; Rachwal, Stanislaw
Liebigs Annalen der Chemie, 1994 , # 1 p. 1 - 6
反应条件
in ethanol
3 h; Heating;
参考文献
Jankowski, Zdzislaw; Stolarski, Roland
Polish Journal of Chemistry, 1980 , vol. 54, # 1 p. 107 - 116
反应条件
iodine; magnesium
1.) THF, reflux, 3 h; 2.) THF, room temp., 6 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Caster, Kenneth C.; Mahni, Fatma; Law, Kam Wah; Rubio, Olga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 781 - 790
反应条件
in diethyl ether
44 h; Heating;
参考文献
Katritzky, Alan R.; Hughes, Craig V.; Rachwal, Stanislaw
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1579 - 1588
反应条件
1: 96 percent / Ambient temperature
2: 73 percent / 120 °C
View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
in diethyl ether
44 h; Heatingother reactants under different reaction conditions; Product distribution;
参考文献
Katritzky, Alan R.; Hughes, Craig V.; Rachwal, Stanislaw
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1579 - 1588